Flüssige Emulsion vom Typ W/O mit AH-Säuren / Liquid emulsion of the W/O type with AH acids
Rezeptur Nr./ Formula no.: 94/081/9a
Bestandteil / Component
%
Funktion/ Function
I.
Monomuls® 90-O 18
Glyceryl Oleate

1,0
W/O-Emulgator/
W/O emulsifier
Dehymuls® HRE 7
PEG-7 Hydrogenated Castor Oil

3,0
W/O-Emulgator/
W/O emulsifier
Cetiol® A
Hexyl Laurate

6,0
Emollient
Cetiol® OE
Dicaprylyl Ether

6,0
Emollient
Cetiol® SN
Cetearyl Isononanoate

7,0
Emollient
Eutanol® G 16
Hexyldecanol

3,0
Emollient
Bienenwachs 8100 (Kahl)
Cera Alba (Beeswax)

1,0
Konsistenzgeber/
consistency giving factor
Zincum N 29 (Bärlocher)
Zinc Stearate

1,0
Stabilisator/stabiliser
II.
Glycolsäure (gepulvert)/Glycolic acid (powder)

0,3
Wirkstoff/active ingredient
DL-Äpfelsäure /DL-Malic acid

0,15
Wirkstoff/active ingredient
L-Weinsäure /L-Tartaric acid

0,15
Wirkstoff/active ingredient
Citronensäure, reinst./
Citric acid, high grade

0,1
Wirkstoff/active ingredient
Milchsäure / Lactic acid approx. 90%

0,32
Wirkstoff/active ingredient
DL-Natriumlactat/ DL-sodium lactate

1,0
Wirkstoff/active ingredient
Natriumpyruvat/sodium pyruvate

0,32
Wirkstoff/active ingredient
Glycerin 86%

5,0
Moisturiser
MgSO4 7H20

1,0
Stabilisator/stabiliser
Aqua

60,71
 
KOH 20%

2,95
Neutralisationsmittel/neutraliser
III.
Konservierungsmittel/preservative

n.B./q.s.
 
pH-Wert (Wasserphase eingestellt)
pH value (aqueous phase adjusted)

5,5
 
Viskosität/viscosity Brookfield RVF, 23� C,
Spindel/rotor 5, 10 UpM/rpm
nach 12 Wochen/ mPas ca.
after 12 weeks mPas approx.

7200



Herstellung im Labormaßstab

1. Komponenten unter I. bei 80 - 85�C schmelzen und homogen vermischen.
2. Komponenten unter II. ebenfalls auf 80 - 85�C erwärmen und unter Rühren/Homogenisieren zu Phase I. geben. 5 Minuten bei Temperatur rühren.
3. Unter weiterem Rühren und Luftkühlung so abkühlen, daß die Emulsion in ständiger homogener Bewegung bleibt und keine Luft eingerührt wird. Bei 60�C homogenisieren (z. B. Ultra Turrax). Intensives Homogenisieren kann zur Erhöhung der Viskosität im Endprodukt führen. Ggf. Kompensation des Wasserverlustes.
4. Emulsion unter Rühren auf 30�C abkühlen lassen.

Preparation in the laboratory

1. Melt the components listed under I at 80-85� C and stir until homogeneous.
2. Heat the components listed under II to 80-85� C and add to phase I while stirring. Stir for 5 min. at this temperature.
3. Allow the emulsion to cool with stirring in such a way that it remains in continual motion. Avoid the incorporation of air. Homogenise at 60� C (e.g.Ultra Turrax). Excessive homogenizing can lead to an increase of the final viscosity. If necessary, compensation of the water loss.
4. Allow the emulsion to cool to 30� C with stirring.



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H E N K E L  K G a A Care Chemicals Division Düsseldorf